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XRD
Equipment Details
Powder X-ray Diffractometer
 
Make: Rigaku Japan
Model: Smart Lab 3 KW 
Target: Cu
Detector: Solid state 2D detector Hypix400
Applications: Phase analysis, Residual stress analysis, Texture analysis
 
 
Charges
 
Type of users Phase analysis charges (INR)* Residual Stress analysis charges (INR)* Texture analysis charges (INR)*
Internal (NIAMT) users 300 300 500
External users (Academic / R&D Institution) 500 500 1500
Industry users 1200 1500 4000

* Prices are for 30 min. slot per sample


SOP for Internal (NIAMT) XRD users (utilizing CPDA fund)

1.Internal (NIAMT) users are required to download the requisition form here based on the type of analysis.

          Requisition Form - Phase Analysis (CPDA User): 
Click here

          Requisition Form - Residual Stress Analysis (CPDA User)Click here

          Requisition Form - Texture Analysis (CPDA User)Click here

2. Fill all the details in the requisition form 

3. Calculate the charges based on the number of samples/number of slots and enter the details in the requisition form.

4. Enter the analysis details in their respective CPDA register and enter the page no. and serial no. details in requisition form.

5. Obtain the signature from supervisor and HOD in requisition form.

6. Attach the duly filled SP-02 form with the requisition form.

7. Submit the requisition form cum SP-02 form along with the samples at the XRD room.
 
8. XRD technician will intimate the completion of analysis to user.

9. User will have to bring the new CD to collect the data. USB Pen drive is strictly not allowed for collection of data.

10. User will have to sign the register book kept in XRD room after the collection of data



SOP for Internal (NIAMT) users

1.Internal (NIAMT) users are required to download the requisition form here based on the type of analysis.

          Requisition Form - Phase Analysis:
Click here

          Requisition Form - Residual Stress Analysis: Click here

          Requisition Form - Texture Analysis: Click here

2. Fill all the details in the requisition form.

3. Obtain the signature from supervisor and HOD.

4. Calculate the charges based on the number of samples/number of slots.

5. Pay the amount by online. The amount once paid is Non-refundable. Payment by any other mode is not accepted.

6. Show the payment transaction details to In-Charge (Accounts) at the accounts section in administrative building.

7. In-Charge (Accounts) will provide money receipt after confirming the transaction details. User may use the money receipt for claiming the reimbursement through CPDA/Project/etc.

8. Attach the copy of money receipt with the XRD requisition form.

9. Fill the ‘details of payment’ in the requisition form.

10. Sign the requisition form.

11. Submit the requisition form along with the samples to the XRD room.

12. XRD technician will intimate the completion of analysis to user.

13. User will have to bring the new CD to collect the data. USB Pen drive is strictly not allowed for collection of data.

14. User will have to sign the register book kept in XRD room after the collection of data. 



SOP for External (Academic / R & D institution /Industry) users

1. External users are required to download the requisition form here based on the type of analysis.

          Requisition Form - Phase Analysis:
Click here

          Requisition Form - Residual Stress Analysis: Click here

          Requisition Form - Texture Analysis: Click here

2. Fill all the details in the requisition form.

3. Obtain the signature from supervisor/HOD (in case of Academic / R & D institution).

4. Calculate the charges based on the number of samples/number of slots.

5. Pay the amount online. The amount once paid is Non-refundable. Payment by any other mode is not accepted. 
 
6. Fill the ‘details of payment’ in the requisition form.

7. Sign the requisition form.

8. Scan the requisition form and send to xrd.cif[at]niamt.ac.in along with the payment transaction details.

9. The payment transaction details will be forwarded to In-Charge (Accounts) at the accounts section – NIAMT.

10. In-Charge (Accounts) will provide a money receipt after confirming the transaction details. A scanned copy of money receipt will be sent to the user. On request, money receipt will also be sent by post to the user’s address. 

11. External users may submit the samples at the XRD room or send the samples by post mentioning in the envelope ‘samples for XRD analysis’ to 

Central Instrument facility, 
National Institute of Advanced Manufacturing Technology (NIAMT), 
Hatia, Ranchi – 834003 Jharkhand
E-mail: cif[at]niamt.ac.in

12. Data will be sent by e-mail to the user or user may bring the new CD to collect the data. USB Pen drive is strictly not allowed for collection of data.

13. In case, external user requires their samples back, they are requested to send a self-addressed envelope with stamp of requisite amount.

14. XRD technician / external user will sign the register book kept in XRD room after the collection of data or after sending the data by e-mail.


 
XRD Lab in-charge:
Dr. H. Vignesh Babu
Assistant Professor
Department of Applied Sciences and Humanities
National Institute of Advanced Manufacturing Technology (NIAMT)
Hatia, Ranchi – 834003
e-mail: xrd.cif[at]niamt.ac.in
    
Visitor No. 105101360704